Titration procedure:
A typical
titration begins with a beaker or Erlenmeyer flask containing
a very precise volume of the analyte and a small amount of indicator (such
as phenolphthalein, Methyl orange, Methyl red etc) placed underneath a
calibrated burette or chemistry pipetting syringe containing
the titrant. Small volumes of the titrant are then added to the analyte drop by
drop until the indicator changes its color in reaction to the titrant
saturation threshold, reflecting arrival at the endpoint of the
titration. Depending on the endpoint desired, single drops or less than a
single drop of the titrant can make the difference between a permanent and
temporary change in the indicator. When the endpoint of the reaction is
reached, the volume of reactant consumed is measured and used to calculate the
concentration of analyte by
Where,
Ct is
the concentration of the titrant, typically in molarity;
Vt is
the volume of the titrant used, typically in liters;
M is the mole ratio of the analyte and reactant from the
balanced chemical equation; and
Va is
the volume of the analyte used, typically in liters.
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